KIMBERLITE INDICATOR MINERAL SORTING
LABORATORY
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Heavy mineral concentrates are hand sorted for kimberlite
indicator minerals in Kitikmeot Geological Ltd.’s sorting laboratory in
North Vancouver B.C. Experienced personnel use binocular microscopes equipped
with the finest Leica optics to examine till sample concentrates for the
minerals that characterize kimberlite. These minerals include purple (chromium-rich)
pyrope garnets, orange eclogitic garnets, emerald green chromium diopside,
olivine, enstatite, picrolimenite, chromite, and diamond. Characteristic
hues, subtle surface features, and unusual shapes are used to distinguish
grains that actually originated in kimberlite from similar minerals derived
from unprospective rock types.
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Quality is assured by daily spiked samples provided
to each sorter.
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All grains tentatively identified by sorters as kimberlite
are confirmed by Kitikmeot Geological’s most experienced sorting supervisors
using more advanced Leica binocular microscopes specially equipped for
petrographic mineral identification. Grains of uncertain origin are mounted
for chemical analysis by electron microprobe.
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Confirmed kimberlite indicator grains are counted and
results entered along with all sample parameters into Kitikmeot Geological’s
computer database, which is linked to sample positions by the head office.
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Pyrope garnet, chrome diopside, olivine, and ilmenite
grains are further examined to classify their surface textures, quantifying
the effects of abrasion and weathering. Characteristic surface textures
including scratch density, fractures, etch pits and kelyphite remnants
are graded using systems developed by Kitikmeot Geological based on in-house
studies of different glacial dispersion trains in northern Canada. These
surface texture grades provide estimates of the distance the grains have
been transported from their kimberlite source.
CAUSTIC FUSION LABORATORY
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Kitikmeot Geological Ltd. operates a large-capacity
caustic fusion laboratory in North Vancouver, British Columbia. The laboratory
runs six 10-kg batches of kimberlite per day at full capacity, and can
process 300 kg per week.
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Each batch is mixed with 100 kg of caustic soda (NaOH)
in specially designed stainless steel alloy buckets, and heated to 600°C
in reinforced kilns. The kiln temperature is raised in stages by a pre-programmed,
computer-controlled protocol to permit maximum reduction of the sample
without damage to any contained microdiamonds. The heating protocol was
developed after extensive in-house experimentation using synthetic diamond
spikes exposed to varied times and temperatures. Synthetic spikes included
with caustic samples verify recover efficiency and the lack of any process-induced
damage to natural diamonds in the sample.
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After heating in the kilns, the hot caustic soda in
poured off and the residue is washed through either 120 or 200 mesh (125
or 75 micron opening) screens, depending on the objectives of each project.
After washing, the caustic residue is cleaned in hydrochloric acid (HCl),
and delivered to Kitikmeot Geological’s secure diamond sorting facility
where it is hand-sorted under binocular microscopes equipped with reflected
and transmitted light stages.
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The recovered diamonds are measured in x-y-z dimensions,
and >1 mm stones are weighed in a 0.1 milligram electronic balance. The
diamonds are then described using Kitikmeot Geological’s in-house grading
system, and all results are entered into our computer data base, where
they can be immediately accessed by geologists and planners in the head
office.
HEAVY MINERAL CONCENTRATE (HMC)
LABORATORY
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Kitikmeot Geological Ltd. operates a heavy mineral concentrate
(HMC) laboratory in North Vancouver, B.C. with the capacity to process
50 to 100 field samples per day. The HMC laboratory is equipped with: three
24 inch automated SWECO sieving units; 6 Wilfley concentrating tables with
attached hopper feeders; 1 permanent (Permaroll) and 2 adjustable (Maglift)
electro-magnetic separators; 3 Franz magnetic separators; 6 Magstreams
with modified collection tubes; and assorted drying racks, hot plates,
and ovens. Concentrates from the laboratory are sorted for kimberlite indicator
minerals, and analyzed for base metal anomalies.
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Samples are first wet sieved into -6/+10, -10/+20, -20/+40,
-40/+50, and -50 mesh fractions using the SWECO sieving units, with all
samples weighed and archived. For kimberlite exploration, the -20/+40 (0.850
to 0.425 mm) fraction is passed over a Wilfley table to produce the initial
heavy mineral concentrate. This concentrate is then divided and reduced
by magnetic separation methods to produce the smallest concentrate possible
for efficient hand-sorting. Magnetic separation starts with separation
of magnetic and non-magnetic fractions using the Permaroll, and production
of highly magnetic and paramagnetic fractions using the Maglifts. The paramagnetic
fraction is split by Magstreams on a combination of density and magnetic
susceptibility into 2 concentrates, 1 containing the silicate kimberlite
indicator minerals, and the other containing oxide indicator minerals.
At this point the original sample has been reduced by 99.8%, and the sample
is ready for hand-sorting.
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Quality is controlled by spiked samples which are run
daily across the Wilfley tables and through each Magstream.
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For base metal exploration, the -50 mesh fraction is
processed. This fraction is passed across the Wilfley table, to produce
a heavy mineral concentrate, which is collected, dried, and weighed. The
HMC is sent to an outside assaying lab for trace element analysis.
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The Kitikmeot Geological HMC laboratory uses non-toxic
and environmentally safe, water based processes to produce a heavy mineral
concentrate. Sieves and concentrating tables operate with only water, Permaroll
and Maglift magnetic separators use no chemicals, and the Magstream uses
only a non-toxic, non-carcinogenic, water soluble suspension of magnetite
in ligno-sulfunate for density separation.
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